浩瀚色谱(山东)应用技术开发有限公司建立便携式气相色谱分析仪快速测定工作场所空气中六氟化硫(SF6)的方法.对质量浓度为0.300~40.000 mg/m3的SF6标准气体最低检出浓度为0.15 mg/m3,准确度为101.0%~104.4%,相对标准偏差为3.7%~4.9%.具有良好的一致性.结论:本法具有良好的准确性和抗干扰性,适用于工作场所空气中SF6水平的现场测定。
名称:填充柱
色谱柱:串连 2 m×4 mm 癸二酸异二辛酯 : Porapak Q = 2 : 100 和 1 m×4 mm 6402 硅胶柱
4.3.1 癸二酸异二辛酯,色谱固定液。
4.3.2 Porapak Q,色谱担体,60 目~80 目。
4.3.3 6402 硅胶,80 目~100 目。
应用:GBZ/T 160.33-2004 工作场所空气中硫化物的测定方法
BZ/T 300.51-2017 工作场所空气有毒物质测定 第51部分:六氟化硫
适用于安捷伦,岛津,赛默飞,瓦里安,布鲁克,PE


Haohan Chromatography (Shandong) Application Technology Development Co., Ltd. has established a portable gas chromatography analyzer for rapid determination of sulfur hexafluoride (SF6) in workplace air The minimum detectable concentration of SF6 standard gas with a mass concentration of 0.300-40.00 mg/m3 is 0.15 mg/m3, with an accuracy of 101.0% -104.4% and a relative standard deviation of 3.7% -4.9% Has good consistency Conclusion: This method has good accuracy and anti-interference properties, and is suitable for on-site determination of SF6 levels in workplace air.
Name: Filler Column
Chromatography column: Tandem 2 m × 4 mm isooctyl sebacate: Porapak Q = 2 : 100 and 1 m × 4 mm 6402 silicone columns
4.3.1 Isodioctyl sebacate, chromatographic stationary phase.
4.3.2 Porapak Q, chromatographic support, 60-80 mesh.
4.3.3 6402 silicone, 80-100 mesh.
Application: GBZ/T 160.33-2004 Determination of Sulfides in Workplace Air
BZ/T 300.51-2017 Determination of Toxic Substances in Workplace Air Part 51: Sulfur Hexafluoride
Suitable for Agilent, Shimadzu, Thermo Fisher, Varian, Brooke, PE
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