浩瀚色谱(山东)应用技术开发有限公司,采用HH-FFAP毛细管柱建立工作场所空气中二硫化碳的气相色谱测定方法。方法:以毛细管柱对被测样品中的二硫化碳进行分离,火焰光度检测器(FPD)进行检测。结果:二硫化碳浓度在0.02μg/ml~6.0μg/ml呈良好的线性关系,相关系数为0.9999;检出限为0.02μg/ml,最低检测浓度为0.03 mg/m3(以采集3.0L空气样品计);相对标准偏差小于5.0%,平均回收率为98%。结论:方法各项指标均符合GBZ/T210.4-2008《职业卫生标准制定指南第4部分:工作场所空气中化学物质测定方法》的要求,适用于工作场所空气中二硫化碳的测定。
名称:毛细管柱
型号:HH-FFAP
规格:30m*0.32mm*0.5um
温度:250°C
应用:GBZ_T300_38-2017工作场所空气有毒物质测定 第38部分二硫化碳
适用于:安捷伦4890,5890,6890,7820,7890,8860,8890
岛津GC-14C,GC-2010,GC-2014,GC-2030
赛默飞1300 ,1310,1600,1610
瓦里安3800
布鲁克,PE580,590,680,690




Haohan Chromatography (Shandong) Application Technology Development Co., Ltd. established a gas chromatography method for the determination of carbon disulfide in workplace air using HH-FFAP capillary column. Method: Carbon disulfide in the tested sample was separated using a capillary column and detected using a flame photometric detector (FPD). Result: The concentration of carbon disulfide showed a good linear relationship between 0.02 μ g/ml and 6.0 μ g/ml, with a correlation coefficient of 0.9999; The detection limit is 0.02 μ g/ml, and the minimum detection concentration is 0.03 mg/m3 (based on collecting 3.0L of air sample); The relative standard deviation is less than 5.0%, and the average recovery rate is 98%. Conclusion: All indicators of the method comply with the requirements of GBZ/T210.4-2008 "Guidelines for the Development of Occupational Health Standards Part 4: Methods for the Determination of Chemical Substances in Workplace Air", and are suitable for the determination of carbon disulfide in workplace air.
Name: Capillary Column
model: HH-FFAP
Specification: 30m * 0.32mm * 0.5um
Temperature: 250 ° C
Application: GBZ_T300_38-2017 Determination of Toxic Substances in Workplace Air Part 38 Carbon Disulfide
Applicable to: Agilent 48905890689078908608890
Shimadzu GC-14C, GC-2010,GC-2014,GC-2030
Thermo Fisher Scientific 130013101601610
Varian 3800
Brooke, PE580,590,680,690
滕州市浩瀚色谱仪器技术服务有限公司
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