浩瀚色谱建立石榴健胃片中桉油精的含量测定方法。方法采用气相色谱(GC)法测定石榴健胃片中桉油精的含量,使用氢火焰离子化检测器检测,检测温度250℃,进样口温度200℃,以高纯度氮气为载气。结果桉油精的回归方程为Y=1 364.478X-5 910.56,r=0.999 2(n=6),表明桉油精在9.05~180.98μg/m L范围内呈良好的线性关系;平均加样回收率为99.69%,RSD为1.43%。结论该法简便、准确、专属性强、重复性好,经方法学验证,本法可用于石榴健胃片中桉油精的含量测定。
名称:10%SE-54不锈钢填充柱
担体:白色硅藻土担体0.17mm-0.25mm
规格:3m*1/8
*高使用温度:300°C
编号:20240423001
应用:安捷伦6890,7890,7820,8860,8890
Establishment of a content determination method for eucalyptol in pomegranate Jianwei tablets using Haohan chromatography. Method: Gas chromatography (GC) was used to determine the content of eucalyptol in pomegranate Jianwei tablets. A hydrogen flame ionization detector was used for detection, with a detection temperature of 250 ℃ and a sample inlet temperature of 200 ℃. High purity nitrogen gas was used as the carrier gas. The regression equation for eucalyptus oil extract is Y=1 364.478X-5 910.56, r=0.999 2 (n=6), indicating that eucalyptus oil extract ranges from 9.05 to 180.98 μ There is a good linear relationship within the range of g/mL; The average sample recovery rate is 99.69%, with an RSD of 1.43%. Conclusion: This method is simple, accurate, highly specific, and has good repeatability. It has been validated by traditional Chinese medicine and can be used for the determination of eucalyptol in pomegranate Jianwei tablets.
Name: 10% SE-54 stainless steel filled column
Support body: white diatomaceous earth support body 0.17mm-0.25mm
Specification: 3m * 1/8
*High operating temperature: 300 ° C
Number: 20240423001
Application: Agilent 68907890782088608890
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