:在r—氧化铝催化剂上,甲醇氯化合成甲胺的反应在下列条件范围——甲醇与氨之比为1:1~2(摩尔比),反应温度400~440℃、气态空速为2000~8000小时,气体线速0.715~3.02厘米/秒,催化剂粒度14~60目,该反应系处于动力学控制区域内。
浩瀚色谱使用蒸馏-气相色谱法测定循环水中氨、甲胺及甲醇的浓度,及时查出生产系统出现的问题。实验证明本方法准确、快速、操作简单,可以在相关行业推广运用。
名称:甲胺填充柱
型号:HH-AM
规格:3m*3mm,60-80目
*高使用温度:120°C
编号:20240227001
应用:工业甲胺,二甲胺,三甲胺的测定 气相色谱法
On the r-alumina catalyst, the reaction of methanol chlorination to synthesize methylamine is carried out under the following conditions: a ratio of methanol to ammonia of 1:1 to 2 (molar ratio), a reaction temperature of 400 to 440 ℃, a gaseous space velocity of 2000 to 8000 hours, a gas linear velocity of 0.715 to 3.02 cm/s, and a catalyst particle size of 14-60 mesh. The reaction system is within the kinetic control region.
Haohan chromatography uses distillation gas chromatography to determine the concentrations of ammonia, methylamine, and methanol in circulating water, and promptly identifies problems in the production system. The experiment proves that this method is accurate, fast, and easy to operate, and can be promoted and applied in related industries.
Name: Methylamine filled column
Model: HH-AM
Specification: 3m * 3mm, 60-80 mesh
*High operating temperature: 120 ° C
Number: 20240227001
Application: Determination of industrial methylamine, dimethylamine, and trimethylamine by gas chromatography
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