浩瀚色谱建立气相色谱法测定氯乙酰氯中二氯乙酰氯的方法.直接进样进行测定.二氯乙酰氯的质量浓度在0.8～2.4 mg/mL范围内与色谱峰峰面积线性关系良好,相关系数为0.9995,方法检出限为8.93μg/mL.样品测定结果的相对标准偏差为2.0％(n=6),加标回收率为103.29％～111.99％.该方法适用于氯乙酰氯中二氯乙酰氯含量的测定.
特点：样品直接进样，不需要转化；柱效高，分离时间短，效率高
名称：毛细管柱
规格：30mm*0.32mm
型号：HHLYS3698-30
最高使用温度：280°C
编号：20231212012
适用于：安捷伦6890,7890,8860,8890；岛津GC-2014，GC-2010，GC-2018，GC-2030；赛默飞，瓦里安，布鲁克，PE等
Establishment of a Gas Chromatography Method for the Determination of Dichloroacetyl Chloride in Chloroacetyl Chloride by Vast Chromatography. Direct Injection for Determination. The mass concentration of Dichloroacetyl chloride in the range of 0.8-2.4 mg/mL has a good linear relationship with the chromatographic peak area, with a correlation coefficient of 0.9995 and a detection limit of 8.93 μ The relative standard deviation of the sample determination results for g/mL is 2.0% (n=6), and the recovery rate for spiking is 103.29%~111.99%. This method is suitable for the determination of dichloroacetyl chloride content in chloroacetyl chloride
Features: The sample is directly injected without the need for conversion; High column efficiency, short separation time, and high efficiency
Name: Capillary Column
Specification: 30mm * 0.32mm
Model: HHLYS3698-30
Maximum operating temperature: 280 ° C
Number: 20231212012
Applicable to: Agilent 6890789088608890; Shimadzu GC-2014, GC-2010, GC-2018, GC-2030; Thermo Fisher, Varian, Brooke, PE, etc
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