碳氢化合物 取本品作为供试品;取甲烷含量为0.0020%的气体(以氮气为稀释剂)作为对照气体,照气相色谱法(通则0521)试验,用玻璃球为填料的色谱柱(0.8m×4mm,80目);柱温为110℃;进样口温度为110℃;检测器温度为120℃。量取供试品气体与对照气体,注入气相色谱仪,在净化温度为360℃时测得的峰面积为相应空白值;量取供试品气体与对照气体,注入气相色谱仪,测定峰面积,减去相应空白值后的峰面积为校正峰面积。按外标法以校正峰面积计算,含碳氢化合物(以甲烷计)不得过0.0020%。
以上是药典二氧化碳的要求,分析的核心部件为净化装置。浩瀚色谱(山东)应用技术开发有限公司,与时俱进,依据药典的要求,研制出HHO-III Purification device二氧化碳专用净化装置,净化效果良好,在制药单位安装测试,效率高,安装简单,无需改造仪器,分析时间短,此款产品为浩瀚色谱的特色产品,欢迎咨询洽谈。
浩瀚色谱,提供详细的分析方案
Take this product as the test sample for hydrocarbons; Take a gas with a methane content of 0.0020% (using nitrogen as the diluent) as the reference gas, and perform the gas chromatography test according to General Rule 0521. Use a chromatographic column (0.8m) filled with glass balls × 4mm, 80 mesh); The column temperature is 110 ℃; The inlet temperature is 110 ℃; The detector temperature is 120 ℃. Measure the test sample gas and control gas, inject them into a gas chromatograph, and the peak area measured at a purification temperature of 360 ℃ is the corresponding blank value; Measure the test sample gas and control gas, inject them into a gas chromatograph, measure the peak area, and subtract the corresponding blank value to obtain the corrected peak area. Calculated using the external standard method to correct peak area, the hydrocarbon content (calculated as methane) shall not exceed 0.0020%.
The above is the requirement for carbon dioxide in the pharmacopoeia, and the core component analyzed is the purification device. Haohan Chromatography (Shandong) Application Technology Development Co., Ltd. is keeping up with the times and according to the requirements of the Pharmacopoeia, has developed the HHO-III Purification device for carbon dioxide purification. The purification effect is good, and it has been installed and tested in pharmaceutical units with high efficiency, simple installation, no need to modify the instrument, and short analysis time. This product is a characteristic product of Haohan Chromatography. Welcome to consult and negotiate.
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